Information card for entry 4066175

Structure parameters

• Formula: C39 H60 Li N2 O3 P
• Calculated formula: C39 H60 Li N2 O3 P
• Title of publication: Carbene-Stabilized Parent Phosphinidene†
• Authors of publication: Wang, Yuzhong; Xie, Yaoming; Abraham, Mariham Y.; Gilliard, Robert J.; Wei, Pingrong; Schaefer, Henry F.; Schleyer, Paul v. R.; Robinson, Gregory H.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 4778
• a: 10.4993 ± 0.0009 Å
• b: 11.3546 ± 0.001 Å
• c: 19.1402 ± 0.0016 Å
• α: 74.097 ± 0.001°
• β: 89.774 ± 0.001°
• γ: 67.732 ± 0.001°
• Cell volume: 2018 ± 0.3 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0988
• Residual factor for significantly intense reflections: 0.0547
• Weighted residual factors for significantly intense reflections: 0.1462
• Weighted residual factors for all reflections included in the refinement: 0.1771
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No