Information card for entry 4066248

Structure parameters

• Formula: C22 H30 Fe O2 Si
• Calculated formula: C22 H30 Fe O2 Si
• Title of publication: Synthesis and Characterization of the Ferrio-Substituted Silicon(II) Compound Me5C5(CO)2FeSiC5Me5†
• Authors of publication: Jutzi, Peter; Leszczyńska, Kinga; Mix, Andreas; Neumann, Beate; Rummel, Britta; Schoeller, Wolfgang; Stammler, Hans-Georg
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 4759
• a: 15.1433 ± 0.0007 Å
• b: 9.2167 ± 0.0004 Å
• c: 30.8421 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4304.7 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0706
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for significantly intense reflections: 0.1024
• Weighted residual factors for all reflections included in the refinement: 0.1144
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No