Information card for entry 4066288

Structure parameters

• Formula: C41 H41 F10 Ge N3
• Calculated formula: C41 H41 F10 Ge N3
• SMILES: [Ge]1(N(C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C)c1c(cccc1C(C)C)C(C)C)N(c1c(F)c(F)c(F)c(F)c1F)c1c(F)c(F)c(F)c(F)c1F
• Title of publication: Isomerization of an N-Heterocyclic Germylene to an Azagermabenzen-1-ylidene and Its Coupling to a Unique Bis(germylene)§
• Authors of publication: Yao, Shenglai; Zhang, Xinhao; Xiong, Yun; Schwarz, Helmut; Driess, Matthias
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 5353
• a: 10.8593 ± 0.0003 Å
• b: 13.1638 ± 0.0004 Å
• c: 14.4489 ± 0.0003 Å
• α: 92.576 ± 0.002°
• β: 101.49 ± 0.002°
• γ: 102.174 ± 0.002°
• Cell volume: 1970.39 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0323
• Residual factor for significantly intense reflections: 0.0264
• Weighted residual factors for significantly intense reflections: 0.0703
• Weighted residual factors for all reflections included in the refinement: 0.0716
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No