Information card for entry 4066289

Structure parameters

• Formula: C64 H94 Ge2 N4
• Calculated formula: C64 H94 Ge2 N4
• Title of publication: Isomerization of an N-Heterocyclic Germylene to an Azagermabenzen-1-ylidene and Its Coupling to a Unique Bis(germylene)§
• Authors of publication: Yao, Shenglai; Zhang, Xinhao; Xiong, Yun; Schwarz, Helmut; Driess, Matthias
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 5353
• a: 11.403 ± 0.003 Å
• b: 14.52 ± 0.002 Å
• c: 18.793 ± 0.003 Å
• α: 78.926 ± 0.012°
• β: 82.882 ± 0.017°
• γ: 78.326 ± 0.016°
• Cell volume: 2978.8 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1041
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for significantly intense reflections: 0.0882
• Weighted residual factors for all reflections included in the refinement: 0.0938
• Goodness-of-fit parameter for all reflections included in the refinement: 0.934
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No