Information card for entry 4066290

Structure parameters

• Formula: C36.34 H50.02 Cl4 O3 Sn
• Calculated formula: C36.34 H50.02 Cl3.99 O3 Sn
• Title of publication: Synthesis and Structure of a Heptacoordinate Trichlorostannane Bearing a Triarylmethyl-Type Tetradentate Ligand†
• Authors of publication: Kobayashi, Junji; Iwanaga, Kohei; Kawashima, Takayuki
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 21
• Pages of publication: 5725
• a: 10.755 ± 0.005 Å
• b: 12.842 ± 0.005 Å
• c: 15.346 ± 0.006 Å
• α: 90.813 ± 0.004°
• β: 98.633 ± 0.006°
• γ: 110.933 ± 0.005°
• Cell volume: 1951.9 ± 1.4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.0291
• Weighted residual factors for significantly intense reflections: 0.0678
• Weighted residual factors for all reflections included in the refinement: 0.0697
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No