Information card for entry 4066934

Structure parameters

• Formula: C30 H72 O3 Si9
• Calculated formula: C30 H72 O3 Si9
• Title of publication: Synthesis and Characterization of {[Tris(trimethylsilyl)silyl]methyl}silanes of the Formula Type Me4−nSi[CH2Si(SiMe3)3]n(n= 1−3) and Derivatives
• Authors of publication: Berkefeld, André; Troegel, Dennis; Burschka, Christian; Tacke, Reinhold
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 20
• Pages of publication: 4548
• a: 10.017 ± 0.002 Å
• b: 26.789 ± 0.004 Å
• c: 10.0531 ± 0.0017 Å
• α: 90°
• β: 118.64 ± 0.02°
• γ: 90°
• Cell volume: 2367.6 ± 0.8 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 4
• Space group number: 6
• Hermann-Mauguin space group symbol: P 1 m 1
• Hall space group symbol: P -2y
• Residual factor for all reflections: 0.0509
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1285
• Weighted residual factors for all reflections included in the refinement: 0.1314
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No