Information card for entry 4067105

Structure parameters

• Formula: C40.5 H37 B Cl F4 N2 O3.5 P2 Rh2
• Calculated formula: C40.5 H37 B Cl F4 N2 O3.5 P2 Rh2
• Title of publication: Dirhodium Complexes Bridged by Bis(diphenylphosphino)phthalazine (PNNPPh): Central Ring Size and Charge Effects As Compared with the Pyrazolate Derivative (PNNPPy)
• Authors of publication: Yamaguchi, Takafumi; Koike, Takashi; Akita, Munetaka
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 23
• Pages of publication: 6493
• a: 11.088 ± 0.001 Å
• b: 12.5827 ± 0.0008 Å
• c: 15.695 ± 0.001 Å
• α: 105.234 ± 0.004°
• β: 93.866 ± 0.004°
• γ: 95.413 ± 0.004°
• Cell volume: 2093.6 ± 0.3 ų
• Cell temperature: 213.2 K
• Ambient diffraction temperature: 213 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for all reflections included in the refinement: 0.1313
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No