Information card for entry 4067106

Structure parameters

• Formula: C76 H66 B2 F8 N4 O5 P4 Rh4
• Calculated formula: C76 H56 B2 F8 N4 O5 P4 Rh4
• Title of publication: Dirhodium Complexes Bridged by Bis(diphenylphosphino)phthalazine (PNNPPh): Central Ring Size and Charge Effects As Compared with the Pyrazolate Derivative (PNNPPy)
• Authors of publication: Yamaguchi, Takafumi; Koike, Takashi; Akita, Munetaka
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 23
• Pages of publication: 6493
• a: 13.375 ± 0.007 Å
• b: 16.02 ± 0.007 Å
• c: 20.37 ± 0.01 Å
• α: 97.3 ± 0.02°
• β: 110.8 ± 0.02°
• γ: 85.28 ± 0.02°
• Cell volume: 4044 ± 3 ų
• Cell temperature: 213.2 K
• Ambient diffraction temperature: 213 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0548
• Weighted residual factors for all reflections included in the refinement: 0.1839
• Goodness-of-fit parameter for all reflections included in the refinement: 0.984
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No