Information card for entry 4067373

Structure parameters

• Chemical name: tris(o-ethoxyphenyl)chlorogermane
• Formula: C24 H27 Cl Ge O3
• Calculated formula: C24 H27 Cl Ge O3
• SMILES: [Ge](Cl)(c1ccccc1OCC)(c1ccccc1OCC)c1ccccc1OCC
• Title of publication: Use of73Ge NMR Spectroscopy and X-ray Crystallography for the Study of Electronic Interactions in Substituted Tetrakis(phenyl)-, -(phenoxy)-, and -(thiophenoxy)germanes
• Authors of publication: Yoder, Claude H.; Agee, Tamara M.; Griffith, Allison K.; Schaeffer, Charles D.; Carroll, Mary J.; DeToma, Alaina S.; Fleisher, Adam J.; Gettel, Cameron J.; Rheingold, Arnold L.
• Journal of publication: Organometallics
• Year of publication: 2010
• Journal volume: 29
• Journal issue: 3
• Pages of publication: 582
• a: 9.2445 ± 0.001 Å
• b: 11.218 ± 0.0012 Å
• c: 23.106 ± 0.003 Å
• α: 94.474 ± 0.002°
• β: 98.982 ± 0.002°
• γ: 106.334 ± 0.002°
• Cell volume: 2252.4 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0571
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.0952
• Weighted residual factors for all reflections included in the refinement: 0.102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No