Information card for entry 4068220

Structure parameters

• Formula: C24 H32 Ga N3 O
• Calculated formula: C24 H32 Ga N3 O
• SMILES: C1(CCCC1)N1c2ccccc2[O]2c3ccccc3N(C3CCCC3)[Ga]12N(C)C
• Title of publication: A Discrete N,O,N-Supported Gallium Amido Complex for the Intermolecular Hydroamination of Terminal Alkynes
• Authors of publication: Hild, Frédéric; Dagorne, Samuel
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 3
• Pages of publication: 1189
• a: 9.9023 ± 0.0004 Å
• b: 11.0556 ± 0.0004 Å
• c: 11.6943 ± 0.0004 Å
• α: 117.631 ± 0.002°
• β: 95.729 ± 0.002°
• γ: 101.957 ± 0.002°
• Cell volume: 1080.91 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0456
• Residual factor for significantly intense reflections: 0.0354
• Weighted residual factors for significantly intense reflections: 0.1
• Weighted residual factors for all reflections included in the refinement: 0.1241
• Goodness-of-fit parameter for all reflections included in the refinement: 1.199
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No