Crystallography Open Database

Information card for entry 4068221

Preview

Coordinates	4068221.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C58 H68 Cl4 Ga2 N6 O2
Calculated formula	C58 H68 Cl4 Ga2 N6 O2
Title of publication	A Discrete N,O,N-Supported Gallium Amido Complex for the Intermolecular Hydroamination of Terminal Alkynes
Authors of publication	Hild, Frédéric; Dagorne, Samuel
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	3
Pages of publication	1189
a	10.7114 ± 0.0005 Å
b	12.016 ± 0.0005 Å
c	12.5614 ± 0.0009 Å
α	113.354 ± 0.001°
β	107.228 ± 0.001°
γ	103.315 ± 0.001°
Cell volume	1301.48 ± 0.13 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0579
Residual factor for significantly intense reflections	0.0449
Weighted residual factors for significantly intense reflections	0.1283
Weighted residual factors for all reflections included in the refinement	0.1357
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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