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Information card for entry 4068244
Preview
Coordinates | 4068244.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H44 Fe P2 Si2 |
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Calculated formula | C24 H44 Fe P2 Si2 |
SMILES | [Fe]12345678(P9[CH]4=[C]3([C]2(=[C]19[Si](C)(C)C(C)(C)C)C)C)P1[CH]8=[C]7([C]6(=[C]51[Si](C)(C)C(C)(C)C)C)C |
Title of publication | Concise Synthesis of Enantiopure (S)-(+)-2,2′-Bis(tert-butyldimethylsilyl)-1,1′-diphosphaferrocene: Anion-Dependence of Its Coordination to Palladium(II) Centers |
Authors of publication | Cabon, Yves; Carmichael, Duncan; Le Goff, Xavier-Frédéric |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 1 |
Pages of publication | 370 |
a | 7.462 ± 0.001 Å |
b | 23.903 ± 0.001 Å |
c | 16.032 ± 0.001 Å |
α | 90° |
β | 108.353 ± 0.001° |
γ | 90° |
Cell volume | 2714.1 ± 0.4 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0709 |
Residual factor for significantly intense reflections | 0.055 |
Weighted residual factors for significantly intense reflections | 0.1349 |
Weighted residual factors for all reflections included in the refinement | 0.1459 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4068244.html
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