Information card for entry 4068245

Structure parameters

• Formula: C106 H156 B2 Cl6 F8 Fe2 N4 P4 Pd4 Si4
• Calculated formula: C105 H154 B2 Cl4 F8 Fe2 N4 P4 Pd4 Si4
• Title of publication: Concise Synthesis of Enantiopure (S)-(+)-2,2′-Bis(tert-butyldimethylsilyl)-1,1′-diphosphaferrocene: Anion-Dependence of Its Coordination to Palladium(II) Centers
• Authors of publication: Cabon, Yves; Carmichael, Duncan; Le Goff, Xavier-Frédéric
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 1
• Pages of publication: 370
• a: 21.022 ± 0.001 Å
• b: 21.022 ± 0.001 Å
• c: 30.883 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 13648 ± 1 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 10
• Space group number: 92
• Hermann-Mauguin space group symbol: P 41 21 2
• Hall space group symbol: P 4abw 2nw
• Residual factor for all reflections: 0.0484
• Residual factor for significantly intense reflections: 0.0445
• Weighted residual factors for significantly intense reflections: 0.1245
• Weighted residual factors for all reflections included in the refinement: 0.1276
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No