Information card for entry 4068276

Structure parameters

• Formula: C24 H31 Au N3 P
• Calculated formula: C24 H31 Au N3 P
• SMILES: [Au]([P](C1CCCCC1)(c1c(c2ccccc2)cccc1)C1CCCCC1)N=N#N
• Title of publication: Facile Synthesis of (Phosphine)- and (N-heterocyclic Carbene)Gold(I) and Silver(I) Azide Complexes
• Authors of publication: Partyka, David V.; Robilotto, Thomas J.; Updegraff, James B.; Zeller, Matthias; Hunter, Allen D.; Gray, Thomas G.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 3
• Pages of publication: 795
• a: 10.2546 ± 0.0004 Å
• b: 10.8364 ± 0.0004 Å
• c: 11.607 ± 0.0004 Å
• α: 62.768 ± 0.002°
• β: 82.646 ± 0.002°
• γ: 75.921 ± 0.002°
• Cell volume: 1112.19 ± 0.07 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0174
• Residual factor for significantly intense reflections: 0.0154
• Weighted residual factors for significantly intense reflections: 0.0357
• Weighted residual factors for all reflections included in the refinement: 0.0376
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No