Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4068277
Preview
Coordinates | 4068277.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H49 Au N3 P |
---|---|
Calculated formula | C33 H49 Au N3 P |
SMILES | [Au]([P](C1CCCCC1)(c1c(cccc1)c1c(cc(cc1C(C)C)C(C)C)C(C)C)C1CCCCC1)N=N#N |
Title of publication | Facile Synthesis of (Phosphine)- and (N-heterocyclic Carbene)Gold(I) and Silver(I) Azide Complexes |
Authors of publication | Partyka, David V.; Robilotto, Thomas J.; Updegraff, James B.; Zeller, Matthias; Hunter, Allen D.; Gray, Thomas G. |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 3 |
Pages of publication | 795 |
a | 18.161 ± 0.003 Å |
b | 17.165 ± 0.003 Å |
c | 22.038 ± 0.004 Å |
α | 90° |
β | 101.12 ± 0.002° |
γ | 90° |
Cell volume | 6741 ± 2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0276 |
Residual factor for significantly intense reflections | 0.023 |
Weighted residual factors for significantly intense reflections | 0.0559 |
Weighted residual factors for all reflections included in the refinement | 0.0572 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.053 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4068277.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.