Information card for entry 4068908

Structure parameters

• Formula: C28 H46 B2 F8 N3 O P2 Rh
• Calculated formula: C28 H46 B2 F8 N3 O P2 Rh
• Title of publication: Synthesis, Structure, and Reactivity of Nitrosyl Pincer-Type Rhodium Complexes
• Authors of publication: Gaviglio, Carina; Ben-David, Yehoshoa; Shimon, Linda J. W.; Doctorovich, Fabio; Milstein, David
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 6
• Pages of publication: 1917
• a: 11.705 ± 0.002 Å
• b: 16.359 ± 0.003 Å
• c: 19.271 ± 0.004 Å
• α: 90°
• β: 98.26 ± 0.03°
• γ: 90°
• Cell volume: 3651.8 ± 1.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0658
• Residual factor for significantly intense reflections: 0.0468
• Weighted residual factors for significantly intense reflections: 0.1266
• Weighted residual factors for all reflections included in the refinement: 0.136
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No