Information card for entry 4068909

Structure parameters

• Formula: C27 H49 B F4 N O P2 Rh
• Calculated formula: C27 H49 B F4 N O P2 Rh
• Title of publication: Synthesis, Structure, and Reactivity of Nitrosyl Pincer-Type Rhodium Complexes
• Authors of publication: Gaviglio, Carina; Ben-David, Yehoshoa; Shimon, Linda J. W.; Doctorovich, Fabio; Milstein, David
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 6
• Pages of publication: 1917
• a: 8.5787 ± 0.0002 Å
• b: 12.6713 ± 0.0004 Å
• c: 15.3075 ± 0.0005 Å
• α: 113.789 ± 0.002°
• β: 97.889 ± 0.002°
• γ: 92.405 ± 0.002°
• Cell volume: 1499.47 ± 0.08 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0647
• Residual factor for significantly intense reflections: 0.0452
• Weighted residual factors for significantly intense reflections: 0.1007
• Weighted residual factors for all reflections included in the refinement: 0.1068
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No