Information card for entry 4068959

Structure parameters

• Formula: C115 H100 B2 Cl2 F40 N4 O2 Si2
• Calculated formula: C115 H100 B2 Cl2 F40 N4 O2 Si2
• Title of publication: From an N-Heterocyclic Silacyclopropene to Donor-Supported Silacyclopropenylium Cations
• Authors of publication: Yao, Shenglai; Xiong, Yun; van Wüllen, Christoph; Driess, Matthias
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 6
• Pages of publication: 1610
• a: 17.2151 ± 0.0004 Å
• b: 16.0582 ± 0.0004 Å
• c: 20.262 ± 0.0005 Å
• α: 90°
• β: 95.557 ± 0.002°
• γ: 90°
• Cell volume: 5575 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1148
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0576
• Weighted residual factors for all reflections included in the refinement: 0.0662
• Goodness-of-fit parameter for all reflections included in the refinement: 0.756
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No