Information card for entry 4068960

Structure parameters

• Common name: C38 H43 Cl2 N3 O2 P2 Pd, 1.4 CH2Cl2
• Formula: C39.4 H43 Cl4.8 N3 O2 P2 Pd
• Calculated formula: C39.4 H43 Cl4.8 N3 O2 P2 Pd
• Title of publication: Diphosphination of Electron Poor Alkenes
• Authors of publication: Hajdók, Imre; Lissner, Falk; Nieger, Martin; Strobel, Sabine; Gudat, Dietrich
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 6
• Pages of publication: 1644
• a: 31.8659 ± 0.0007 Å
• b: 15.3565 ± 0.0004 Å
• c: 20.4915 ± 0.0004 Å
• α: 90°
• β: 124.458 ± 0.001°
• γ: 90°
• Cell volume: 8268.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0768
• Residual factor for significantly intense reflections: 0.0556
• Weighted residual factors for significantly intense reflections: 0.1057
• Weighted residual factors for all reflections included in the refinement: 0.1138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No