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Information card for entry 4069054
Preview
Coordinates | 4069054.cif |
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Original paper (by DOI) | HTML |
Formula | C32 H44 Cl2 N3 O V |
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Calculated formula | C32 H44 Cl2 N3 O V |
SMILES | [V]12(Cl)(Cl)(OC(c3[n]1c(ccc3)C(=[N]2c1c(cccc1C(C)C)C(C)C)C)(C)C)=NC12CC3CC(C1)CC(C2)C3 |
Title of publication | Synthesis of (1-Adamantylimido)vanadium(V)-alkyl Complexes Containing a Chelate Alkoxo(imino)pyridine Ligand, and Reactions with Alcohols (ROH) That Proceed via Intermediates Formed by Coordination of ROH |
Authors of publication | Zhang, Wenjuan; Katao, Shohei; Sun, Wen-Hua; Nomura, Kotohiro |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 5 |
Pages of publication | 1558 |
a | 10.1796 ± 0.0004 Å |
b | 10.6325 ± 0.0005 Å |
c | 17.056 ± 0.0006 Å |
α | 102.298 ± 0.0017° |
β | 91.9098 ± 0.0013° |
γ | 114.248 ± 0.0015° |
Cell volume | 1629.37 ± 0.12 Å3 |
Cell temperature | 193.1 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for significantly intense reflections | 0.0625 |
Weighted residual factors for all reflections included in the refinement | 0.1118 |
Goodness-of-fit parameter for all reflections included in the refinement | 1 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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