Information card for entry 4069055

Structure parameters

• Formula: C60 H84 N5 O2 Si V
• Calculated formula: C60 H84 N5 O2 Si V
• Title of publication: Synthesis of (1-Adamantylimido)vanadium(V)-alkyl Complexes Containing a Chelate Alkoxo(imino)pyridine Ligand, and Reactions with Alcohols (ROH) That Proceed via Intermediates Formed by Coordination of ROH
• Authors of publication: Zhang, Wenjuan; Katao, Shohei; Sun, Wen-Hua; Nomura, Kotohiro
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 5
• Pages of publication: 1558
• a: 16.5172 ± 0.0016 Å
• b: 16.9839 ± 0.0015 Å
• c: 21.2017 ± 0.0018 Å
• α: 90°
• β: 97.306 ± 0.002°
• γ: 90°
• Cell volume: 5899.4 ± 0.9 ų
• Cell temperature: 193.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0681
• Weighted residual factors for all reflections included in the refinement: 0.1715
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No