Information card for entry 4069056

Structure parameters

• Formula: C85 H112 F12 N6 O4 Si2 V2
• Calculated formula: C85 H112 F12 N6 O4 Si2 V2
• Title of publication: Synthesis of (1-Adamantylimido)vanadium(V)-alkyl Complexes Containing a Chelate Alkoxo(imino)pyridine Ligand, and Reactions with Alcohols (ROH) That Proceed via Intermediates Formed by Coordination of ROH
• Authors of publication: Zhang, Wenjuan; Katao, Shohei; Sun, Wen-Hua; Nomura, Kotohiro
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 5
• Pages of publication: 1558
• a: 11.7792 ± 0.001 Å
• b: 14.5592 ± 0.0012 Å
• c: 16.3464 ± 0.0014 Å
• α: 64.162 ± 0.002°
• β: 77.042 ± 0.002°
• γ: 77.02 ± 0.002°
• Cell volume: 2433 ± 0.4 ų
• Cell temperature: 193.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0676
• Weighted residual factors for all reflections included in the refinement: 0.0772
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No