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Information card for entry 4069339
Preview
Coordinates | 4069339.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C39 H56 N2 Si |
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Calculated formula | C39 H56 N2 Si |
SMILES | [Si@@]123(N(C(=C[C@]3([C@]32([C@@]1(C(=C)C(=C3C)C)C)C)C)C)c1c(cccc1C(C)C)C(C)C)Nc1c(cccc1C(C)C)C(C)C.[Si@]123(N(C(=C[C@@]3([C@@]32([C@]1(C(=C)C(=C3C)C)C)C)C)C)c1c(cccc1C(C)C)C(C)C)Nc1c(cccc1C(C)C)C(C)C |
Title of publication | Reaction of the (Pentamethylcyclopentadienyl)silicon(II) Cation with a Sterically Encumbered β-Diketiminato Anion: Unexpected Formation of a Tricyclic Silicon(IV) Compound |
Authors of publication | Jutzi, Peter; Leszczyńska, Kinga; Mix, Andreas; Neumann, Beate; Schoeller, Wolfgang W.; Stammler, Hans-Georg |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 7 |
Pages of publication | 1985 |
a | 11.1676 ± 0.0003 Å |
b | 11.2054 ± 0.0002 Å |
c | 14.1174 ± 0.0003 Å |
α | 92.5007 ± 0.0014° |
β | 100.875 ± 0.0011° |
γ | 93.9357 ± 0.0014° |
Cell volume | 1727.91 ± 0.07 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0467 |
Residual factor for significantly intense reflections | 0.0386 |
Weighted residual factors for significantly intense reflections | 0.0946 |
Weighted residual factors for all reflections included in the refinement | 0.1012 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069339.html
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Users of the data should acknowledge the original authors of the
structural data.