Information card for entry 4069340

Structure parameters

• Formula: C33 H51 Li N2 O2
• Calculated formula: C34 H51 Li N2 O2
• Title of publication: Reaction of the (Pentamethylcyclopentadienyl)silicon(II) Cation with a Sterically Encumbered β-Diketiminato Anion: Unexpected Formation of a Tricyclic Silicon(IV) Compound
• Authors of publication: Jutzi, Peter; Leszczyńska, Kinga; Mix, Andreas; Neumann, Beate; Schoeller, Wolfgang W.; Stammler, Hans-Georg
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 7
• Pages of publication: 1985
• a: 14.4427 ± 0.0005 Å
• b: 21.3898 ± 0.0005 Å
• c: 10.4885 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3240.18 ± 0.18 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0801
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1289
• Weighted residual factors for all reflections included in the refinement: 0.1488
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No