Information card for entry 4069539

Structure parameters

• Formula: C25 H51 B F4 Os P2
• Calculated formula: C25 H51 B F4 Os P2
• Title of publication: Trapping of a 12-Valence-Electron Osmium Intermediate
• Authors of publication: Buil, María L.; Esteruelas, Miguel A.; Garcés, Karin; García-Raboso, Jorge; Oliván, Montserrat
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 15
• Pages of publication: 4606
• a: 8.571 ± 0.0003 Å
• b: 10.5741 ± 0.0005 Å
• c: 15.5455 ± 0.0005 Å
• α: 79.513 ± 0.003°
• β: 84.033 ± 0.003°
• γ: 88.269 ± 0.003°
• Cell volume: 1377.77 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0391
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for significantly intense reflections: 0.0582
• Weighted residual factors for all reflections included in the refinement: 0.0596
• Goodness-of-fit parameter for all reflections included in the refinement: 0.975
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No