Information card for entry 4069540

Structure parameters

• Formula: C36 H91 B F4 Os2 P4
• Calculated formula: C36 H91 B F4 Os2 P4
• Title of publication: Trapping of a 12-Valence-Electron Osmium Intermediate
• Authors of publication: Buil, María L.; Esteruelas, Miguel A.; Garcés, Karin; García-Raboso, Jorge; Oliván, Montserrat
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 15
• Pages of publication: 4606
• a: 17.14 ± 0.004 Å
• b: 15.568 ± 0.004 Å
• c: 17.737 ± 0.004 Å
• α: 90°
• β: 99.757 ± 0.004°
• γ: 90°
• Cell volume: 4664.4 ± 1.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for significantly intense reflections: 0.0469
• Weighted residual factors for all reflections included in the refinement: 0.0497
• Goodness-of-fit parameter for all reflections included in the refinement: 0.827
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No