Information card for entry 4069610

Structure parameters

• Chemical name: Bis{(u-n2-hydridodiethylgermyl)tetracarbonylmolybdenum(I)}
• Formula: C16 H22 Ge2 Mo2 O8
• Calculated formula: C8 H11 Ge Mo O4
• Title of publication: Photochemical Reaction of Mo(CO)6with Et2GeH2: NMR and DFT Studies of Reaction Products; Crystal Structure of a Novel Complex [{Mo(μ-η2-H−GeEt2)(CO)4}2]
• Authors of publication: Zyder, Magdalena; Kochel, Andrzej; Handzlik, Jarosław; Szymańska-Buzar, Teresa
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 20
• Pages of publication: 5857
• a: 9.183 ± 0.002 Å
• b: 10.109 ± 0.002 Å
• c: 14.233 ± 0.002 Å
• α: 90°
• β: 120.82 ± 0.02°
• γ: 90°
• Cell volume: 1134.7 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0238
• Residual factor for significantly intense reflections: 0.0185
• Weighted residual factors for significantly intense reflections: 0.0426
• Weighted residual factors for all reflections included in the refinement: 0.0441
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No