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Information card for entry 4069611
Preview
Coordinates | 4069611.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H26 Cl4 N2 Pd |
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Calculated formula | C33 H26 Cl4 N2 Pd |
SMILES | [Pd]1(Cl)([n]2c3c([N]41Cc1ccc5ccccc5c1c1c5ccccc5ccc1C4)cccc3ccc2)C.C(Cl)(Cl)Cl |
Title of publication | Application of Chiral Amine-Imine Ligands in Palladium-Catalyzed Polyketone Synthesis: Effect of Ligand Backbone on the Polymer Stereochemistry |
Authors of publication | Axet, M. Rosa; Amoroso, Francesco; Bottari, Giovanni; D’Amora, Angela; Zangrando, Ennio; Faraone, Felice; Drommi, Dario; Saporita, Maria; Carfagna, Carla; Natanti, Paolo; Seraglia, Roberta; Milani, Barbara |
Journal of publication | Organometallics |
Year of publication | 2009 |
Journal volume | 28 |
Journal issue | 15 |
Pages of publication | 4464 |
a | 8.25 ± 0.003 Å |
b | 20.859 ± 0.004 Å |
c | 9.051 ± 0.003 Å |
α | 90° |
β | 110.62 ± 0.03° |
γ | 90° |
Cell volume | 1457.8 ± 0.8 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.144 |
Residual factor for significantly intense reflections | 0.0621 |
Weighted residual factors for significantly intense reflections | 0.1353 |
Weighted residual factors for all reflections included in the refinement | 0.16 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.822 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4069611.html
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