Information card for entry 4069700

Structure parameters

• Formula: C37 H48 Cl N Nb P Rh
• Calculated formula: C37 H48 Cl N Nb P Rh
• Title of publication: Niobium/Rhodium Bimetallic Complexes: Synthesis, Structure, and Catalytic Hydrosilylation of Acetophenone and Benzaldehyde
• Authors of publication: Leelasubcharoen, Somying; Zhizhko, Pavel A.; Kuzmina, Lyudmila G.; Churakov, Andrei V.; Howard, Judith A. K.; Nikonov, Georgii I.
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 15
• Pages of publication: 4500
• a: 9.1766 ± 0.0006 Å
• b: 18.6877 ± 0.0012 Å
• c: 20.1635 ± 0.0012 Å
• α: 90°
• β: 98.312 ± 0.003°
• γ: 90°
• Cell volume: 3421.5 ± 0.4 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.087
• Residual factor for significantly intense reflections: 0.0587
• Weighted residual factors for significantly intense reflections: 0.105
• Weighted residual factors for all reflections included in the refinement: 0.1113
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No