Information card for entry 4070387

Structure parameters

• Formula: C8.62 H25.23 Hf0.62 N1.85 O0.62 Si2.46
• Calculated formula: C8.61538 H25.2308 Hf0.615385 N1.84615 O0.615385 Si2.46154
• Title of publication: Reactions of Oxygen with Metallaheterocyclic Alkyl Amide Complexes. Selective Insertion of Oxygen into Metal−Carbon Bonds
• Authors of publication: Yu, Xianghua; Chen, Xue-Tai; Xue, Zi-Ling
• Journal of publication: Organometallics
• Year of publication: 2009
• Journal volume: 28
• Journal issue: 23
• Pages of publication: 6642
• a: 15.09 ± 0.004 Å
• b: 17.812 ± 0.005 Å
• c: 18.071 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4857 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0361
• Residual factor for significantly intense reflections: 0.0309
• Weighted residual factors for significantly intense reflections: 0.0776
• Weighted residual factors for all reflections included in the refinement: 0.0826
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No