Information card for entry 4070714

Structure parameters

• Formula: C55 H66 N3 P Rh Si4 Sn
• Calculated formula: C55 H66 N3 P Rh Si4 Sn
• Title of publication: Triamidostannates(II) as Sterically Demanding Ligands for Rhodium and Iridium
• Authors of publication: Kilian, Michaela; Wadepohl, Hubert; Gade, Lutz H.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 4
• Pages of publication: 524
• a: 11.87 ± 0.003 Å
• b: 11.947 ± 0.002 Å
• c: 19.451 ± 0.005 Å
• α: 85.419 ± 0.005°
• β: 81.054 ± 0.004°
• γ: 81.686 ± 0.004°
• Cell volume: 2691.5 ± 1.1 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0376
• Weighted residual factors for significantly intense reflections: 0.0692
• Weighted residual factors for all reflections included in the refinement: 0.0744
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No