Information card for entry 4070713

Structure parameters

• Formula: C53 H65 N3 P Rh Si4 Sn
• Calculated formula: C53 H65 N3 P Rh Si4 Sn
• SMILES: [CH]12=[CH]3C4[CH]5=[CH](C1C4)[Rh]235([P](c1ccccc1)(c1ccccc1)c1ccccc1)[Sn]12N(c3ccc(cc3)C)[Si](C)(C)[Si](C)([Si](C)(C)N1c1ccc(cc1)C)[Si](C)(C)N2c1ccc(cc1)C
• Title of publication: Triamidostannates(II) as Sterically Demanding Ligands for Rhodium and Iridium
• Authors of publication: Kilian, Michaela; Wadepohl, Hubert; Gade, Lutz H.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 4
• Pages of publication: 524
• a: 42.049 ± 0.004 Å
• b: 12.9598 ± 0.0011 Å
• c: 19.6423 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10704 ± 1.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0844
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for significantly intense reflections: 0.1259
• Weighted residual factors for all reflections included in the refinement: 0.1366
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No