Crystallography Open Database

Information card for entry 4070830

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Coordinates	4070830.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H66 B F24 N3 Pd
Calculated formula	C66 H66 B F24 N3 Pd
Title of publication	Reactions of Cationic Palladium α-Diimine Complexes with Nitrogen-Containing Olefins: Branched Polyethylene with Carbazole Functionalities
Authors of publication	Li, Weidong; Zhang, Xiaochun; Meetsma, Auke; Hessen, Bart
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	9
Pages of publication	2052
a	41.414 ± 0.002 Å
b	12.7965 ± 0.0005 Å
c	26.01 ± 0.001 Å
α	90°
β	103 ± 0.001°
γ	90°
Cell volume	13430.8 ± 1 Å³
Cell temperature	100 ± 1 K
Ambient diffraction temperature	100 ± 1 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0989
Residual factor for significantly intense reflections	0.0618
Weighted residual factors for significantly intense reflections	0.1468
Weighted residual factors for all reflections included in the refinement	0.1664
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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