Information card for entry 4070831

Structure parameters

• Formula: C78 H71 B F24 N3 Pd
• Calculated formula: C78 H71 B F24 N3 Pd
• Title of publication: Reactions of Cationic Palladium α-Diimine Complexes with Nitrogen-Containing Olefins: Branched Polyethylene with Carbazole Functionalities
• Authors of publication: Li, Weidong; Zhang, Xiaochun; Meetsma, Auke; Hessen, Bart
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 9
• Pages of publication: 2052
• a: 12.8846 ± 0.0006 Å
• b: 15.727 ± 0.0007 Å
• c: 36.571 ± 0.002 Å
• α: 90°
• β: 91.951 ± 0.001°
• γ: 90°
• Cell volume: 7406.3 ± 0.6 ų
• Cell temperature: 100 ± 1 K
• Ambient diffraction temperature: 100 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0969
• Residual factor for significantly intense reflections: 0.0762
• Weighted residual factors for significantly intense reflections: 0.1932
• Weighted residual factors for all reflections included in the refinement: 0.2061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No