Information card for entry 4071187

Structure parameters

• Formula: C18 H27 Cl Os
• Calculated formula: C18 H27 Cl Os
• Title of publication: Synthesis and Protonation Studies of Cp*Os(dppe)H: Kinetic versus Thermodynamic Control
• Authors of publication: Dub, Pavel A.; Belkova, Natalia V.; Lyssenko, Konstantin A.; Silantyev, Gleb A.; Epstein, Lina M.; Shubina, Elena S.; Daran, Jean-Claude; Poli, Rinaldo
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 13
• Pages of publication: 3307
• a: 14.18 ± 0.003 Å
• b: 13.87 ± 0.002 Å
• c: 16.468 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3238.9 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0719
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.096
• Weighted residual factors for all reflections included in the refinement: 0.1173
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No