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Information card for entry 4071188
Preview
Coordinates | 4071188.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H40 Os P2 |
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Calculated formula | C36 H40 Os P2 |
Title of publication | Synthesis and Protonation Studies of Cp*Os(dppe)H: Kinetic versus Thermodynamic Control |
Authors of publication | Dub, Pavel A.; Belkova, Natalia V.; Lyssenko, Konstantin A.; Silantyev, Gleb A.; Epstein, Lina M.; Shubina, Elena S.; Daran, Jean-Claude; Poli, Rinaldo |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 13 |
Pages of publication | 3307 |
a | 15.584 ± 0.003 Å |
b | 15.643 ± 0.003 Å |
c | 12.747 ± 0.003 Å |
α | 90° |
β | 101.54 ± 0.03° |
γ | 90° |
Cell volume | 3044.7 ± 1.1 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0386 |
Residual factor for significantly intense reflections | 0.0296 |
Weighted residual factors for significantly intense reflections | 0.0697 |
Weighted residual factors for all reflections included in the refinement | 0.0745 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.023 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4071188.html
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