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Information card for entry 4071983
Preview
Coordinates | 4071983.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C70 H50 Yb |
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Calculated formula | C70 H50 Yb |
SMILES | c1ccccc1[c]12[Yb]3456789([c]([c]28c2ccccc2)([c]3([c]15c1ccccc1)c1ccccc1)c1ccccc1)[c]1([c]9([c]7([c]6([c]41c1ccccc1)c1ccccc1)c1ccccc1)c1ccccc1)c1ccccc1 |
Title of publication | Accessing Decaphenylmetallocenes of Ytterbium, Calcium, and Barium by Desolvation of Solvent-Separated Ion Pairs: Overcoming Adverse Solubility Properties# |
Authors of publication | Deacon, Glen B.; Forsyth, Craig M.; Jaroschik, Florian; Junk, Peter C.; Kay, Danielle L.; Maschmeyer, Thomas; Masters, Anthony F.; Wang, Jun; Field, Leslie D. |
Journal of publication | Organometallics |
Year of publication | 2008 |
Journal volume | 27 |
Journal issue | 18 |
Pages of publication | 4772 |
a | 10.346 ± 0.0002 Å |
b | 13.4649 ± 0.0003 Å |
c | 18.1324 ± 0.0004 Å |
α | 90° |
β | 95.586 ± 0.001° |
γ | 90° |
Cell volume | 2513.99 ± 0.09 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 3 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0618 |
Residual factor for significantly intense reflections | 0.0302 |
Weighted residual factors for significantly intense reflections | 0.0647 |
Weighted residual factors for all reflections included in the refinement | 0.0741 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.04 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4071983.html
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