Accessing Decaphenylmetallocenes of Ytterbium, Calcium, and Barium by Desolvation of Solvent-Separated Ion Pairs: Overcoming Adverse Solubility Properties#
Authors of publication
Deacon, Glen B.; Forsyth, Craig M.; Jaroschik, Florian; Junk, Peter C.; Kay, Danielle L.; Maschmeyer, Thomas; Masters, Anthony F.; Wang, Jun; Field, Leslie D.
Journal of publication
Organometallics
Year of publication
2008
Journal volume
27
Journal issue
18
Pages of publication
4772
a
14.1148 ± 0.0002 Å
b
14.143 ± 0.0002 Å
c
24.0136 ± 0.0006 Å
α
79.845 ± 0.001°
β
75.352 ± 0.001°
γ
88.167 ± 0.001°
Cell volume
4564.87 ± 0.15 Å3
Cell temperature
123 ± 2 K
Ambient diffraction temperature
123 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.088
Residual factor for significantly intense reflections
0.0516
Weighted residual factors for significantly intense reflections
0.1006
Weighted residual factors for all reflections included in the refinement
0.113
Goodness-of-fit parameter for all reflections included in the refinement
