Information card for entry 4072076

Structure parameters

• Formula: C25 H34 Cl O P2 Rh Si2
• Calculated formula: C25 H34 Cl O P2 Rh Si2
• Title of publication: Synthesis, Properties, and Catalytic Applications of Caged, Compact Trialkylphosphine 4-Phenyl-1-phospha-4-silabicyclo[2.2.2]octane
• Authors of publication: Ochida, Atsuko; Hamasaka, Go; Yamauchi, Yoshihiro; Kawamorita, Soichiro; Oshima, Naoya; Hara, Kenji; Ohmiya, Hirohisa; Sawamura, Masaya
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 21
• Pages of publication: 5494
• a: 6.914 ± 0.004 Å
• b: 6.698 ± 0.004 Å
• c: 28.42 ± 0.02 Å
• α: 90°
• β: 95.71 ± 0.04°
• γ: 90°
• Cell volume: 1309.6 ± 1.4 ų
• Cell temperature: 110.2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0419
• Weighted residual factors for all reflections included in the refinement: 0.0938
• Goodness-of-fit parameter for all reflections included in the refinement: 3.25
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No