Information card for entry 4072077

Structure parameters

• Formula: C32 H54 P2 Pt Si2
• Calculated formula: C29 H47 P2 Pt Si2
• Title of publication: Synthesis, Properties, and Catalytic Applications of Caged, Compact Trialkylphosphine 4-Phenyl-1-phospha-4-silabicyclo[2.2.2]octane
• Authors of publication: Ochida, Atsuko; Hamasaka, Go; Yamauchi, Yoshihiro; Kawamorita, Soichiro; Oshima, Naoya; Hara, Kenji; Ohmiya, Hirohisa; Sawamura, Masaya
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 21
• Pages of publication: 5494
• a: 11.626 ± 0.001 Å
• b: 18.686 ± 0.002 Å
• c: 14.094 ± 0.002 Å
• α: 90°
• β: 101.368 ± 0.002°
• γ: 90°
• Cell volume: 3001.8 ± 0.6 ų
• Cell temperature: 123.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0743
• Weighted residual factors for all reflections included in the refinement: 0.1044
• Goodness-of-fit parameter for all reflections included in the refinement: 3.313
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No