Information card for entry 4072118

Structure parameters

• Formula: C22 H56 B2 P2 Pb Si2
• Calculated formula: C22 H56 B2 P2 Pb Si2
• Title of publication: Agostic-Type B−H···Pb Interactions Stabilize a Dialkylplumbylene. Structure of and Bonding in [{nPr2P(BH3)}(Me3Si)C(CH2)]2Pb
• Authors of publication: Izod, Keith; McFarlane, William; Wills, Corinne; Clegg, William; Harrington, Ross W.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 17
• Pages of publication: 4386
• a: 11.4623 ± 0.0008 Å
• b: 14.0466 ± 0.0012 Å
• c: 22.4174 ± 0.0015 Å
• α: 101.861 ± 0.001°
• β: 93.528 ± 0.001°
• γ: 114.037 ± 0.001°
• Cell volume: 3183.1 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0328
• Residual factor for significantly intense reflections: 0.0246
• Weighted residual factors for significantly intense reflections: 0.0571
• Weighted residual factors for all reflections included in the refinement: 0.0607
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No