Information card for entry 4072155

Structure parameters

• Formula: C32 H44 N U
• Calculated formula: C32 H39 N U
• SMILES: [U]123456789(N(c%10c9cccc%10)c9ccccc9)([c]9([c]1([c]8([c]2([c]39C)C)C)C)C)[c]1([c]4([c]5([c]6([c]71C)C)C)C)C
• Title of publication: A Mild Protocol To Generate Uranium(IV) Mixed-Ligand Metallocene Complexes using Copper(I) Iodide
• Authors of publication: Graves, Christopher R.; Schelter, Eric J.; Cantat, Thibault; Scott, Brian L.; Kiplinger, Jaqueline L.
• Journal of publication: Organometallics
• Year of publication: 2008
• Journal volume: 27
• Journal issue: 20
• Pages of publication: 5371
• a: 9.2465 ± 0.0009 Å
• b: 10.885 ± 0.0011 Å
• c: 13.7791 ± 0.0014 Å
• α: 86.5926 ± 0.0014°
• β: 80.0815 ± 0.0014°
• γ: 80.0828 ± 0.0015°
• Cell volume: 1345.1 ± 0.2 ų
• Cell temperature: 120 ± 1 K
• Ambient diffraction temperature: 120 ± 1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0441
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0842
• Weighted residual factors for all reflections included in the refinement: 0.0875
• Goodness-of-fit parameter for all reflections included in the refinement: 0.826
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No