Crystallography Open Database

Information card for entry 4072286

Preview

Coordinates	4072286.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26.5 H36 Cl3 N3 Ru
Calculated formula	C26.5 H36 Cl3 N3 Ru
Title of publication	Unsymmetrical Bis(iminoethyl)pyridine Metal Complexes with a Pendant Alkenyl Substituent. Part B: Internal Olefin Coordination to Ruthenium†
Authors of publication	Wallenhorst, Carolin; Kehr, Gerald; Fröhlich, Roland; Erker, Gerhard
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	24
Pages of publication	6557
a	25.836 ± 0.001 Å
b	10.897 ± 0.001 Å
c	19.487 ± 0.001 Å
α	90°
β	96.4 ± 0.01°
γ	90°
Cell volume	5452.1 ± 0.6 Å³
Cell temperature	198 ± 2 K
Ambient diffraction temperature	198 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0611
Residual factor for significantly intense reflections	0.0544
Weighted residual factors for significantly intense reflections	0.1472
Weighted residual factors for all reflections included in the refinement	0.1548
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4072286.html