Crystallography Open Database

Information card for entry 4072287

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Coordinates	4072287.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27.5 H38 Cl3 N3 Ru
Calculated formula	C27.5 H38 Cl3 N3 Ru
Title of publication	Unsymmetrical Bis(iminoethyl)pyridine Metal Complexes with a Pendant Alkenyl Substituent. Part B: Internal Olefin Coordination to Ruthenium†
Authors of publication	Wallenhorst, Carolin; Kehr, Gerald; Fröhlich, Roland; Erker, Gerhard
Journal of publication	Organometallics
Year of publication	2008
Journal volume	27
Journal issue	24
Pages of publication	6557
a	25.8516 ± 0.0005 Å
b	10.8712 ± 0.0002 Å
c	20.0594 ± 0.0003 Å
α	90°
β	94.351 ± 0.001°
γ	90°
Cell volume	5621.2 ± 0.17 Å³
Cell temperature	198 ± 2 K
Ambient diffraction temperature	198 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0565
Residual factor for significantly intense reflections	0.0421
Weighted residual factors for significantly intense reflections	0.0941
Weighted residual factors for all reflections included in the refinement	0.1
Goodness-of-fit parameter for all reflections included in the refinement	1.146
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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