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Information card for entry 4073238
Preview
Coordinates | 4073238.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C19 H27 Fe2 N O3 Si3 |
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Calculated formula | C19 H27 Fe2 N O3 Si3 |
SMILES | [Fe]123456([Fe]789%10([Si]%111C[Si](N%11[Si](C)(C)C)(C)C)(C2=O)(C#[O])[cH]1[cH]%10[cH]9[cH]8[cH]71)(C#[O])[cH]1[cH]6[cH]5[cH]4[cH]31 |
Title of publication | Photochemical Reaction of CpFe(CO)2SiMe3(Cp = η5-C5H5) with a Trihydrosilane Containing a Bulky Amino Substituent, Bis(trimethylsilyl)aminosilane |
Authors of publication | Hirotsu, Masakazu; Nishida, Takuo; Sasaki, Hiromitsu; Muraoka, Takako; Yoshimura, Takashi; Ueno, Keiji |
Journal of publication | Organometallics |
Year of publication | 2007 |
Journal volume | 26 |
Journal issue | 10 |
Pages of publication | 2495 |
a | 8.404 ± 0.0005 Å |
b | 17.3179 ± 0.0008 Å |
c | 15.7939 ± 0.0011 Å |
α | 90° |
β | 101.368 ± 0.002° |
γ | 90° |
Cell volume | 2253.5 ± 0.2 Å3 |
Cell temperature | 113 ± 2 K |
Ambient diffraction temperature | 113 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.053 |
Residual factor for significantly intense reflections | 0.0521 |
Weighted residual factors for significantly intense reflections | 0.1331 |
Weighted residual factors for all reflections included in the refinement | 0.1346 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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