Information card for entry 4073239

Structure parameters

• Formula: C39 H80 Fe3 N3 O3 Si9
• Calculated formula: C39 H73 Fe3 N3 O3 Si9
• Title of publication: Photochemical Reaction of CpFe(CO)2SiMe3(Cp = η5-C5H5) with a Trihydrosilane Containing a Bulky Amino Substituent, Bis(trimethylsilyl)aminosilane
• Authors of publication: Hirotsu, Masakazu; Nishida, Takuo; Sasaki, Hiromitsu; Muraoka, Takako; Yoshimura, Takashi; Ueno, Keiji
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 10
• Pages of publication: 2495
• a: 12.313 ± 0.0004 Å
• b: 12.4321 ± 0.0002 Å
• c: 18.7094 ± 0.0005 Å
• α: 72.974 ± 0.003°
• β: 84.917 ± 0.004°
• γ: 77.009 ± 0.004°
• Cell volume: 2667.56 ± 0.13 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0491
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.1254
• Weighted residual factors for all reflections included in the refinement: 0.1408
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No