Information card for entry 4073261

Structure parameters

• Formula: C25 H6 N2 O19 Os7
• Calculated formula: C25 H6 N2 O19 Os7
• SMILES: [Os]12345([Os]6789([Os]1([n]1c(N%1049[Os]492([Os]26%10([Os]374([Os]82(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])(C9=O)(C#[O])C#[O])(C5=O)(C#[O])C#[O])cccc1C)(C#[O])(C#[O])C#[O])(C#[O])C#[O])(C#[O])C#[O]
• Title of publication: High-Nuclearity Osmium Carbonyl Cluster Complexes Containing (6-Methylpyrid-2-yl)imido Ligands. Synthesis of Hepta-, Octa-, and Nonanuclear Derivatives
• Authors of publication: Cabeza, Javier A.; del Río, Ignacio; García-Álvarez, Pablo; Miguel, Daniel
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 13
• Pages of publication: 3212
• a: 10.708 ± 0.005 Å
• b: 10.761 ± 0.005 Å
• c: 17.276 ± 0.007 Å
• α: 101.42 ± 0.008°
• β: 94.927 ± 0.008°
• γ: 114.891 ± 0.007°
• Cell volume: 1737.7 ± 1.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1006
• Residual factor for significantly intense reflections: 0.0869
• Weighted residual factors for significantly intense reflections: 0.2222
• Weighted residual factors for all reflections included in the refinement: 0.2411
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No