Information card for entry 4073262

Structure parameters

• Formula: C26 H8 N2 O20 Os8
• Calculated formula: C26 H8 N2 O20 Os8
• SMILES: c12cccc(C)[n]2[Os]2(C#[O])(C#[O])(C#[O])[Os]34567(C#[O])(C#[O])N891[Os]1%10%1123(C#[O])(C#[O])[Os]23%129(C(=O)[Os]9482(C#[O])(C#[O])[Os]2513(C#[O])(C#[O])([Os]%10%12(C#[O])(C#[O])(C#[O])[H]2)([Os]69(C#[O])(C#[O])C#[O])[H]7%11)(C#[O])C#[O]
• Title of publication: High-Nuclearity Osmium Carbonyl Cluster Complexes Containing (6-Methylpyrid-2-yl)imido Ligands. Synthesis of Hepta-, Octa-, and Nonanuclear Derivatives
• Authors of publication: Cabeza, Javier A.; del Río, Ignacio; García-Álvarez, Pablo; Miguel, Daniel
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 13
• Pages of publication: 3212
• a: 16.9899 ± 0.0001 Å
• b: 11.8232 ± 0.0008 Å
• c: 18.983 ± 0.0001 Å
• α: 90°
• β: 103.28 ± 0.001°
• γ: 90°
• Cell volume: 3711.2 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0352
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0728
• Weighted residual factors for all reflections included in the refinement: 0.0934
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No