Information card for entry 4073263

Structure parameters

• Formula: C31 H14 Cl2 N4 O19 Os9
• Calculated formula: C31 H14 Cl2 N4 O19 Os9
• SMILES: [Os]12345([Os]6789([Os]%10%11([Os]%12%13%14%15([Os]%16%17%181([Os]26%10%12([Os]37%11%13%16[O])(C#[O])([N]59c1[n]([Os]48(C#[O])(C#[O])C#[O])c(ccc1)C)[N]%15%18c1[n]([Os]%14%17(C#[O])(C#[O])C#[O])c(ccc1)C)(C#[O])C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])(C#[O])C#[O])(C#[O])C#[O].C(Cl)Cl
• Title of publication: High-Nuclearity Osmium Carbonyl Cluster Complexes Containing (6-Methylpyrid-2-yl)imido Ligands. Synthesis of Hepta-, Octa-, and Nonanuclear Derivatives
• Authors of publication: Cabeza, Javier A.; del Río, Ignacio; García-Álvarez, Pablo; Miguel, Daniel
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 13
• Pages of publication: 3212
• a: 10.383 ± 0.004 Å
• b: 11.184 ± 0.005 Å
• c: 20.07 ± 0.008 Å
• α: 97.207 ± 0.008°
• β: 93.225 ± 0.008°
• γ: 91.379 ± 0.008°
• Cell volume: 2307.4 ± 1.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0482
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.1093
• Weighted residual factors for all reflections included in the refinement: 0.1175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No