Information card for entry 4073286

Structure parameters

• Formula: C20 H48 O11 P3 Re Sn
• Calculated formula: C20 H48 O11 P3 Re Sn
• SMILES: [Re](C#[O])(C#[O])([SnH3])([P](OCC)(OCC)OCC)([P](OCC)(OCC)OCC)[P](OCC)(OCC)OCC
• Title of publication: Preparation and Reactivity of Stannyl Complexes of Manganese and Rhenium
• Authors of publication: Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; García-Fontán, Soledad; Zanardo, Gianluigi
• Journal of publication: Organometallics
• Year of publication: 2007
• Journal volume: 26
• Journal issue: 11
• Pages of publication: 2918
• a: 17.267 ± 0.003 Å
• b: 11.6003 ± 0.0018 Å
• c: 18.095 ± 0.003 Å
• α: 90°
• β: 112.887 ± 0.003°
• γ: 90°
• Cell volume: 3339.1 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0557
• Weighted residual factors for all reflections included in the refinement: 0.0597
• Goodness-of-fit parameter for all reflections included in the refinement: 0.85
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No